3-(2-萘基氧基)-1-丙醇合成路线 (共 22 条)
反应条件
1.1: sodium carbonate / acetonitrile / 72 h / 80 °C / Inert atmosphere
2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 20 °C / Inert atmosphere
2.2: 0 - 20 °C / Inert atmosphere
3.1: N-iodo-succinimide / dichloromethane / -78 - 20 °C / Inert atmosphere
4.1: C19H20N4 / N,N-dimethyl-formamide; mineral oil / 18 h / 110 °C / Inert atmosphere
View Scheme
参考文献
Sword, Ryan; Baldwin, Luke A.; Murphy, John A.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 9 p. 3560 - 3570
反应条件
pyridine; thionyl chloride
参考文献
Kirner; Richter
Journal of the American Chemical Society, 1929 , vol. 51, p. 3414