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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
75983-90-3
合成路线
（共 8 条）
75983-90-3
→
反应条件
24851-98-7
二氢茉莉酮酸甲酯
反应条件
1: 83 percent 2: 87 percent / PPh3 / Pd(OAc)2 / various solvent(s) / 3 h / Heating 3: 88 percent / NaI / hexamethylphosphoric acid triamide / 100 °C 4: 9-BBN 5: CrO3 View Scheme
参考文献
Tsuji, Jiro; Kobayashi, Yuichi; Kataoka, Hideaki; Takahashi, Takashi
Tetrahedron Letters, 1980 , vol. 21, p. 1475 - 1478
75983-90-3
→
反应条件
3572-64-3
二氢茉莉酸
反应条件
1: 83 percent 2: 87 percent / PPh3 / Pd(OAc)2 / various solvent(s) / 3 h / Heating 3: 88 percent / NaI / hexamethylphosphoric acid triamide / 100 °C 4: 9-BBN 5: CrO3 View Scheme
参考文献
Tsuji, Jiro; Kobayashi, Yuichi; Kataoka, Hideaki; Takahashi, Takashi
Tetrahedron Letters, 1980 , vol. 21, p. 1475 - 1478
75983-90-3
→
反应条件
64670-13-9
+
75351-18-7
+
75351-19-8
反应条件
triphenylphosphine; palladium diacetate in tetrahydrofuran 8 h; Heating; Yield given;
参考文献
Tsuji, Jiro; Kobayashi, Yuichi; Kataoka, Hideaki; Takahashi, Takashi
Tetrahedron Letters, 1980 , vol. 21, p. 1475 - 1478
75983-90-3
→
反应条件
75351-19-8
反应条件
1: PPh3 / Pd(OAc)2 / acetonitrile / 1 h / Heating 2: PPh3 / Pd(OAc)2 / acetonitrile / 1 h View Scheme
参考文献
Tsuji, Jiro; Kobayashi, Yuichi; Kataoka, Hideaki; Takahashi, Takashi
Tetrahedron Letters, 1980 , vol. 21, p. 1475 - 1478
75983-90-3
→
反应条件
64670-13-9
+
75351-19-8
反应条件
triphenylphosphine; palladium diacetate in acetonitrile 1 h; Heatingother solvents, phosphines or phosphites and times; Product distribution;
参考文献
Tsuji, Jiro; Kobayashi, Yuichi; Kataoka, Hideaki; Takahashi, Takashi
Tetrahedron Letters, 1980 , vol. 21, p. 1475 - 1478
75983-90-3
→
反应条件
64670-13-9
+
75351-18-7
+
75351-19-8
反应条件
triphenylphosphine; palladium diacetate in tetrahydrofuran 8 h; Heating; Yield given;
参考文献
Tsuji, Jiro; Kobayashi, Yuichi; Kataoka, Hideaki; Takahashi, Takashi
Tetrahedron Letters, 1980 , vol. 21, p. 1475 - 1478
75983-90-3
→
反应条件
64670-13-9
反应条件
1: PPh3 / Pd(OAc)2 / acetonitrile / 1 h / Heating 2: N-methylpyrrolidone / 6 h / 195 °C View Scheme
参考文献
Tsuji, Jiro; Kobayashi, Yuichi; Kataoka, Hideaki; Takahashi, Takashi
Tetrahedron Letters, 1980 , vol. 21, p. 1475 - 1478
75983-90-3
→
反应条件
64670-13-9
+
75351-19-8
反应条件
triphenylphosphine; palladium diacetate in acetonitrile 1 h; Heatingother solvents, phosphines or phosphites and times; Product distribution;
参考文献
Tsuji, Jiro; Kobayashi, Yuichi; Kataoka, Hideaki; Takahashi, Takashi
Tetrahedron Letters, 1980 , vol. 21, p. 1475 - 1478
