5-溴-N-(3-甲氧基苯基)-2-糠酰胺合成路线 （共 3 条）
反应条件
4-(N,N-dimethlyamino)pyridine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in N,N-dimethyl-formamide
T=25°C; 14 h;
参考文献
THE UNIVERSITY OF TENNESSEE RESEARCH FOUNDATION; COLORADO STATE UNIVERSITY RESEARCH FOUNDATION
Patent: WO2005/7625 A2, 2005 ;
Location in patent: Page 44 ;
反应条件
4-(N,N-dimethlyamino)pyridine in N,N-dimethyl-formamide
参考文献
University of Tennessee Research Foundation
Patent: US2005/222408 A1, 2005 ;
反应条件
1: thiophenol With sodium hydride in N,N-dimethyl-formamide
T=0°C; 0.25 h;
2: 5-bromofuran-2-carboxylic acid (3-methoxyphenyl)amide in N,N-dimethyl-formamide
T=150°C; 12 h;
参考文献
THE UNIVERSITY OF TENNESSEE RESEARCH FOUNDATION; COLORADO STATE UNIVERSITY RESEARCH FOUNDATION
Patent: WO2005/7625 A2, 2005 ;
Location in patent: Page 45-46 ;
