反应条件
1: 93 percent / toluene / 2.5 h / Heating
2: 8.7 g / sodium hydroxide (20percent) / 60 °C
6: 28.8 g / fluoroboric acid, sodium nitrite / H2O
7: 7.6 g / warming, distillation
8: 1.) lithium / 1.) ether, 2 h
9: Cu-quinoline
10: boron tribromide, pyridine hydrochloride / CH2Cl2 / 24 h / -78 °C
View Scheme
参考文献
Durrani, Aziz A.; Tyman, John H. P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1658 - 1666
