cobalt(III) acetate; lithium bromide 24 h; Ambient temperaturevar. time, var. conc., insted of Co(Ac)3 Mn(Ac)3 was used, without halide, presence of water; Product distributionMechanism;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 21, # 8 p. 1445 - 1452
Zhurnal Organicheskoi Khimii, , vol. 21, # 8 p. 1585 - 1592
in chloroform byproducts: H2O; suspn. of trans-OsO2(AsPh3)2Cl2 and CF3COOH in chloroform refluxed for 2h; excess solvent distilled off from react. mixt.; residue dissolved in CHCl3; complex pptd. with hexane; complex dried in vac. over KOH; elem. anal.;
参考文献
Belyaev; Eremin; Simanova; Evreinova
Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya, 2004 , vol. 30, # 4 p. 262 - 268