anhydrous potassium trifluoroacetate in water; acetonitrile T=25°C; electrochemical reaction, total electricity of 0.082 F, the anode was platinum gauze, the cathode was made of GC-2000 glassy carbon. The current density was 33 mA cm-2.; Yield given. Yields of byproduct given;
参考文献
Grinberg; Lundgren; Sterlin; Mysov
Russian Chemical Bulletin, 1997 , vol. 46, # 6 p. 1131 - 1135
in trifluoroacetic acid ZnO was stirred in CF3COOH at room temp. for 2 h; excess CF3COOH was removed under vac., washed with Et2O and dried in vac. at 50°C overnight;
in n-heptane byproducts: H2O; (N2); addn. of ZnO to a soln. of anhydride and acid in heptane, stirringfor 24 h at room temp.; filtration, drying in vac.; elem. anal.;
