in tetrachloromethane
aliquots of CF3COOH (ca. 0.1 equiv) were added to a soln. of the stannane in CCl4 in a NMR tube containing cyclohexane as a reference, reactionwas monitored by (1)H NMR spectroscopy; reactions were rapid and complete before the spectrum was obtained; not isolated, identified by (1)H NMR spectrum;
参考文献
Cuthberston, Matthew J.; Hawker, Darryl W.; Wells, Peter R.
Journal of Organometallic Chemistry, 1985 , vol. 287, p. 7 - 24
