1: isopropenylbenzene With PyBH2I in dichloromethane T=20°C; 2 h; 2: With sodium hydroxide; water in dichloromethane T=0 - 20°C; 3: 2,3-dimethylbutane-2,3-diol in dichloromethane; water T=20°C; 15 h;
参考文献
Karatjas, Andrew G.; Vedejs, Edwin
Journal of Organic Chemistry, 2008 , vol. 73, # 23 p. 9508 - 9510
1.1: n-butyllithium / diethyl ether / 1.5 h / -78 - 10 °C 1.2: 16 h / -10 - 20 °C 2.1: n-butyllithium / tetrahydrofuran / 16 h / -78 °C 3.1: hydrogenchloride / diethyl ether / 0 °C View Scheme
参考文献
Putty, Sandeep; Rai, Aman; Jamindar, Darshan; Pagano, Paul; Quinn, Cheryl L.; Mima, Takehiko; Schweizer, Herbert P.; Gutheil, William G.
Chemical Biology and Drug Design, 2011 , vol. 78, # 5 p. 757 - 763
