反应条件
1: 3-bromo-5-(2-methoxyethoxy)pyridine With n-butyllithium in diethyl ether; hexane T=-80°C; Inert atmosphere; 2: With boric acid trimethyl ester in diethyl ether; hexane T=-80 - 20°C; 12 h; Inert atmosphere; 3: 2,3-dimethylbutane-2,3-diol With acetic acid in diethyl ether; hexane T=20°C; 6 h; Inert atmosphere;
参考文献
Li, Zhiou; Kishi, Norifumi; Hasegawa, Kimiko; Akita, Munetaka; Yoshizawa, Michito
Chemical Communications, 2011 , vol. 47, # 30 p. 8605 - 8607