Howard et al.
Journal of Research of the National Bureau of Standards (United States), 1947 , vol. 38, p. 391
Chem. Zentralbl., 1947 , vol. 118, p. 5291
1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane
under inert atmosphere, standard Schlenk and vac. line techniques; react. between Pt complex and pinacol in the presence of DBU in CH2Cl2; monitored by NMR spectroscopy;
参考文献
Lu, Norman; Norman, Nicholas C.; Guy Orpen; Quayle, Michael J.; Timms, Peter L.; Whittell, George R.
Journal of the Chemical Society, Dalton Transactions, 2000 , # 22 p. 4032 - 4037
1: tBuCH2CH2B(H)NiPr2; 3,4,5-(MeO)3C6H2N2BF4 With biscyclopentadienyliron(II) in acetonitrile
T=20°C; 2.5 h;
2: With methanol in acetonitrile
T=0 - 20°C; 1 h;
3: 2,3-dimethylbutane-2,3-diol in diethyl ether; acetonitrile
T=20°C; 4 h; Reagent/catalyst;
参考文献
UNIVERSITE DE BORDEAUX 1; CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE; PUCHEAULT, Mathieu Jonathan Damien; MARCIASINI, Ludovic Daniel Alain; VAULTIER, Michel
Patent: WO2014/9169 A1, 2014 ;
Location in patent: Page/Page column 56 ;