triethylamine in dichloromethane
T=20°C; 1.25 h; Inert atmosphere;
参考文献
Del Grosso, Alessandro; Helm, Matthew D.; Solomon, Sophia A.; Caras-Quintero, Dolores; Ingleson, Michael J.
Chemical Communications, 2011 , vol. 47, # 46 p. 12459 - 12461
in dichloromethane; dichloromethane-d2
using standard Schlenk techniques; Et3N in CD2Cl2-CH2Cl2 treated with B compd. and AlCl3; treated with N-methylindole for 3 h; treated with Et3Nand pinacol; rotated for 30 min; solvent removed under vac.; dried for 1 h; hexane added; filtered; hexane removed from filtrate under vac.; dried overnight; monitored by (1)H and (11)B NMR spectra;
参考文献
Solomon; Del Grosso; Clark; Bagutski; McDouall; Ingleson
Organometallics, 2012 , vol. 31, # 5 p. 1908 - 1916