1,1,1,2-四氯-2,2-二氟乙烷合成路线 (共 60 条)
反应条件
T=450 - 475°C; durch photochemische Chlorierung;
参考文献
Iikubo, Yuichi; Hedrick, Vicki; Brandstadter, Stephen M.; Cohn, Mitchel
Patent: US2004/127757 A1, 2004 ;
Location in patent: Page 6-7 ;
反应条件
aluminium trichloride in 1,2,2-trifluoro-trichloroethane T=45°C; 9 h;
参考文献
Paleta, Oldrich; Liska, Frantisek; Posta, Antonin; Dedek, Vaclav
Collection of Czechoslovak Chemical Communications, 1980 , vol. 45, # 1 p. 104 - 114
反应条件
fluorine in CF3O-CFCl-CF2Cl T=-30°C; 3 h; Product distribution / selectivity;
参考文献
SOLVAY SOLEXIS S.p.A.
Patent: US2007/203368 A1, 2007 ;
Location in patent: Page/Page column 5 ;
反应条件
aluminium trichloride; iodine; iodine cloride T=35 - 40°C;
参考文献
Hauptschein,M. et al.
Journal of the American Chemical Society, 1961 , vol. 83, p. 2495 - 2500
反应条件
aluminium trichloride in tetrachloromethane T=55 - 74°C; 5.5 h;
参考文献
Okuhara,K.
Journal of Organic Chemistry, 1978 , vol. 43, p. 2745 - 2749
反应条件
aluminium trichloride
参考文献
Miller
Journal of the American Chemical Society, 1940 , vol. 62, p. 993
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Bernstein; Miller
Journal of the American Chemical Society, 1940 , vol. 62, p. 949
反应条件
T=200°C; bei der Photochlorierung;
参考文献
McBee; Bolt
Industrial and Engineering Chemistry, 1947 , vol. 39, p. 412,413
反应条件
aluminium trichloride in carbon disulfide 20.5 h; Heating;
参考文献
Okuhara,K.
Journal of Organic Chemistry, 1978 , vol. 43, p. 2745 - 2749
参考文献
Hauptschein,M. et al.
Journal of the American Chemical Society, 1961 , vol. 83, p. 2495 - 2500
反应条件
aluminum tri-bromide in cyclohexane
参考文献
Okuhara,K.
Journal of Organic Chemistry, 1978 , vol. 43, p. 2745 - 2749