1,2,3-三氯五氟丙烷合成路线 (共 26 条)
参考文献
Journal of the American Chemical Society, , vol. 72, p. 705
反应条件
zinc in methanol
T=50°C; 2 h; Yield given. Yields of byproduct given;
参考文献
Paleta, Oldrich; Kvicala, Jaroslav; Guenter, Jaroslav; Dedek, Vaclav
Bulletin de la Societe Chimique de France, 1986 , # 6 p. 920 - 924
反应条件
phosphorous acid trisdiethylamide in benzonitrile
ice-salt bath;
参考文献
Montanari, Vittorio; DesMarteau, Darryl D.
Journal of Organic Chemistry, 1992 , vol. 57, # 18 p. 5018 - 5019
反应条件
zinc in methanol
T=50°C; 2 h; Yield given. Yields of byproduct given;
参考文献
Paleta, Oldrich; Kvicala, Jaroslav; Guenter, Jaroslav; Dedek, Vaclav
Bulletin de la Societe Chimique de France, 1986 , # 6 p. 920 - 924
反应条件
triethylsilane; meta-chloroperoxybenzoic acid
1) 25 deg C, 1 h, 2) 100 deg C, 12 h; Yield givenFurther byproducts given. Yields of byproduct given;
参考文献
Petrov, Viacheslav A.
Journal of Organic Chemistry, 1998 , vol. 63, # 21 p. 7294 - 7297
反应条件
triethylsilane; meta-chloroperoxybenzoic acid
1) 25 deg C, 1 h, 2) 100 deg C, 12 h; Yield givenFurther byproducts given. Yields of byproduct given;
参考文献
Petrov, Viacheslav A.
Journal of Organic Chemistry, 1998 , vol. 63, # 21 p. 7294 - 7297