2,2-二甲基-1,3-丁二醇合成路线 （共 14 条）
反应条件
sulfuric acid Heating; Further byproducts given;
参考文献
Mazet,M.; Desmaison-Brut,M.
Bulletin de la Societe Chimique de France, 1971 , p. 2656 - 2662
反应条件
nickel
T=70°C; P=73550.8 Torr; Hydrogenation;
参考文献
Kelso et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 287,292
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Hellier, Desmond G.; Phillips, Andrew M.
Organic Magnetic Resonance, 1982 , vol. 18, # 3 p. 178 - 184
反应条件
lithium aluminium tetrahydride
参考文献
Virtanen, Terttu; Nikander, Hannu
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1982 , vol. 36, # 2 p. 113 - 116
反应条件
sodium hydroxide; sodium tetrahydroborate in tetrahydrofuran
2.5 h;
参考文献
Hoffmann, Reinhard W.; Ditrich, Klaus; Froech, Sybille
Liebigs Annalen der Chemie, 1987 , p. 977 - 986
参考文献
Fossek; Swoboda
Monatshefte fuer Chemie, 1890 , vol. 11, p. 389
反应条件
in n-heptane; dichloromethane
16 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Balasubramaniam, Rajiv P.; Moss, David K.; Wyatt, Justin K.; Spence, John D.; Gee, Arvin; Nantz, Michael H.
Tetrahedron, 1997 , vol. 53, # 22 p. 7429 - 7444
反应条件
sodium periodate
1.) CH2Cl2, heptane, room temp., 16 h, 2.) THF, H2O (1:1), room temp., 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Balasubramaniam, Rajiv P.; Moss, David K.; Wyatt, Justin K.; Spence, John D.; Gee, Arvin; Nantz, Michael H.
Tetrahedron, 1997 , vol. 53, # 22 p. 7429 - 7444
参考文献
Franke; Kohn
Monatshefte fuer Chemie, 1906 , vol. 27, p. 1101
参考文献
Franke; Kohn
Monatshefte fuer Chemie, 1906 , vol. 27, p. 1101
