2,2,3,3-四氟丙醇合成路线 （共 89 条）
反应条件
sodium hydroxide in 1,4-dioxane T=50°C; 1 h;
参考文献
Mizukado, Junji; Matsukawa, Yasuhisa; Quan, Heng-Dao; Tamura, Masanori; Sekiya, Akira
Journal of Fluorine Chemistry, 2006 , vol. 127, # 3 p. 400 - 404
反应条件
sodium sulfate in acetonitrile T=50°C; 2 h;
参考文献
Journal of Fluorine Chemistry, , vol. 44, p. 433 - 440
反应条件
(i) Cl2, (ii) aq. KOH; Multistep reaction;
参考文献
Brace,N.O.
Journal of Organic Chemistry, 1961 , vol. 26, p. 4005 - 4010
反应条件
electrochemical reaction;
参考文献
Maksimov, B. N.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 12 p. 1935 - 1940
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 12 p. 1838 - 1842
反应条件
sulfuric acid; hydroquinone in benzene Heating;
参考文献
Boutevin, B.; Rigal, G.; Rousseau, A.; Bosc, D.
Journal of Fluorine Chemistry, 1988 , vol. 38, p. 47 - 74
反应条件
aniline; phosphorus trichoride in diethyl ether T=-35 - -30°C; var. temp., var. ratio of reagent; Product distribution;
参考文献
Konovalova, I. V.; Burnaeva, L. A.; Khusnutdinova, E. K.; Khafizova, G. S.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 10 p. 2189 - 2194,1943 - 1947
反应条件
phosphorus tribromide in neat (no solvent) 20 deg C, 1 h; 50-60 deg C, 45 h; Product distribution;
参考文献
Krolevets, A. A.; Ragulin, L. I.; Shevchenko, V. I.; Lyubimova, E. I.
J. Gen. Chem. USSR (Engl. Transl.), 1986 , vol. 56, # 3 p. 584 - 588,516 - 520
反应条件
oxygen; vanadium pentoxide; silica gel T=350°C; 4 h;
参考文献
Kharchuk; Shishmakov; Volkov; Petrov
Russian Journal of Organic Chemistry, 1998 , vol. 34, # 2 p. 284 - 285
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 53, # 9 p. 1945 - 1950,1754 - 1758
反应条件
pyridine in diethyl ether
参考文献
PPG Industries, Inc.
Patent: US4022609 A1, 1977 ;
