2,2,3,3-四氟丙醇合成路线 （共 89 条）
反应条件
sodium sulfate in acetonitrile T=50°C; 2 h;
参考文献
Journal of Fluorine Chemistry, , vol. 44, p. 433 - 440
反应条件
Cadmium acetate T=185°C; 5 h; various reagents(potassium alkoxides and hydroxide); various solvents, amount reagents, complexing additives, reaction time; Product distribution;
参考文献
Trofimov, B. A.; Khil'ko, M. Ya.; Nedolya, N. A.; Demanov, Yu. K.; Vyalykh, E. P.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 647 - 651
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 4 p. 744 - 749
反应条件
triethylamine in diethyl ether T=20°C; 2 h;
参考文献
Snegirev, V. F.; Makarov, K. N.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 1 p. 91 - 103
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 1 p. 106 - 119
反应条件
N,N-dimethylamino-1,1,2,2-tetrafluoroethane T=170°C; 12 h;
参考文献
Petrov; Swearingen; Hong; Chris Petersen
Journal of Fluorine Chemistry, 2001 , vol. 109, # 1 p. 25 - 31
反应条件
ammonia; tetra-n-propylammonium bromide in water T=0 - 6°C; 5 h; Product distribution / selectivity;
参考文献
JP2005/314356 A, ;
Page/Page column 10-11; 13 ;
反应条件
triethylamine T=4.3 - 10.2°C; 2.5 h; Neat (no solvent); Product distribution / selectivity;
参考文献
JP2005/314356 A, ;
Page/Page column 14-15 ;
反应条件
T=150 - 180°C; Product distribution;
参考文献
Svoboda, Jiri; Paleta, Oldrich; Liska, Frantisek; Dedek, Vaclav
Collection of Czechoslovak Chemical Communications, 1981 , vol. 46, # 6 p. 1389 - 1396
反应条件
50percent iger natronlauge; tetrabutyl-ammonium chloride T=40°C; 10 h; other α,α',ω-trihydroperfluoroalcoholes, other reagents; var. solvents; var. times and temp.; Product distribution;
参考文献
Sonnek, Georg; Rabe, Christiane; Schmaucks, Gerd; Kaden, Reinfried; Lehms, Ingeburg
Journal of Organometallic Chemistry, 1991 , vol. 405, # 2 p. 179 - 182
反应条件
chlorine; triphenylphosphine in tetrachloromethane Heating;
参考文献
Zapevalov, A. Yu.; Saloutina, L. V.; Kodess, M. I.; Kolenko, I. P.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 8 p. 1466 - 1472
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 8 p. 1626 - 1633
反应条件
T=150 - 180°C; Product distribution;
参考文献
Svoboda, Jiri; Paleta, Oldrich; Liska, Frantisek; Dedek, Vaclav
Collection of Czechoslovak Chemical Communications, 1981 , vol. 46, # 6 p. 1389 - 1396
