2,2,3,3-四氟丙醇合成路线 （共 89 条）
反应条件
sodium hydroxide; CuCl2 in 2-methyl-propan-1-ol
参考文献
Hoechst Aktiengesellschaft
Patent: US5495034 A1, 1996 ;
反应条件
sodium dichromate; sulfuric acid
参考文献
Atherton,J.H. et al.
Journal of the Chemical Society [Section] C: Organic, 1971 , p. 366 - 371
反应条件
triethylamine T=5 - 20°C; 5 h;
参考文献
Russian Journal of General Chemistry, , vol. 64, # 8.1 p. 1162 - 1163
Zhurnal Obshchei Khimii, , vol. 64, # 8 p. 1292 - 1293
反应条件
triethylamine T=5 - 20°C;
参考文献
Studnev, Yu. N.; Kinosh, O. F.; Zabornya, V. V.; Frolovskii, V. A.; Stolyarov, V. P.; Rozantsev, G. G.
Russian Journal of General Chemistry, 1994 , vol. 64, # 8.1 p. 1162 - 1163
Zhurnal Obshchei Khimii, 1994 , vol. 64, # 8 p. 1292 - 1293
反应条件
triethylamine T=5 - 20°C;
参考文献
Studnev, Yu. N.; Kinosh, O. F.; Zabornya, V. V.; Frolovskii, V. A.; Stolyarov, V. P.; Rozantsev, G. G.
Russian Journal of General Chemistry, 1994 , vol. 64, # 8.1 p. 1162 - 1163
Zhurnal Obshchei Khimii, 1994 , vol. 64, # 8 p. 1292 - 1293
反应条件
hydroquinone; sulfonated coal; sulfuric acid in benzene T=80°C; 10 h;
参考文献
Gol'din; Averbakh; Nekrasova; Lavygin; Leitan; Chalbysheva
Journal of applied chemistry of the USSR, 1985 , vol. 58, # 6 pt 2 p. 1244 - 1247
反应条件
potassium hydroxide in water T=75 - 95°C; P=5625.56 - 6000.6 Torr; 8.5 h; Inert atmosphereAutoclave; Product distribution / selectivity;
参考文献
Daikin Industries, Ltd.
Patent: EP2305626 A1, 2011 ;
Location in patent: Page/Page column 6-8; 11 ;
反应条件
triethylamine in dichloromethane T=-40°C; 0.5 h;
参考文献
Ofitserov, E. N.; Mironov, V. F.; Sinyashina, T. N.; Konovalova, I. V.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1990 , vol. 60, # 1.1. p. 39 - 49,33 - 42
反应条件
hydrogen fluoride; boron trifluoride T=150°C; Etherification; 14 h;
参考文献
Petrov, Viacheslav A.; Davidson, Fred
Journal of Fluorine Chemistry, 1999 , vol. 95, # 1-2 p. 5 - 14
反应条件
(i), (ii) SF4; Multistep reaction;
参考文献
Aldrich,P.E.; Sheppard,W.A.
Journal of Organic Chemistry, 1964 , vol. 29, p. 11 - 15
