2,2,3,3-四氟丙醇合成路线 （共 89 条）
反应条件
triethylamine in diethyl ether 2 h;
参考文献
Mironov, V. F.; Konovalova, I. V.; Mavleev, R. A.; Mukhtarov, A. Sh.; Ofitserov, E. N.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1991 , vol. 61, # 10 p. 2150 - 2154,1997 - 2001
反应条件
sodium hydroxide; tetreamethyl ammonium hydroxide T=50°C; 5 h;
参考文献
Solov'ev, D. V.; Kolomenskaya, L. V.; Rodin, A. A.; Zenkevich, I. G.; Lavrent'ev, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1991 , vol. 61, # 3.2 p. 673 - 678,611 - 615
反应条件
triethylamine in diethyl ether T=20°C; 2.5 h;
参考文献
Konovalova, I. V.; Ofitserov, E. N.; Sinyashina, T. N.; Mironov, V. F.; Pudovik, A. N.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1987 , vol. 36, p. 1078 - 1081
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1987 , vol. 36, # 5 p. 1164 - 1167
反应条件
potassium hydroxide in water
T=50 - 60°C; P=3000.3 - 3750.38 Torr; Inert atmosphereAutoclave;
参考文献
Daikin Industries, Ltd.
Patent: EP2305626 A1, 2011 ;
Location in patent: Page/Page column 12-13 ;
反应条件
potassium hydroxide in bis [2-(2-methoxyethoxy)ethyl] ether; water
T=35°C; P=1500.15 Torr;
参考文献
ASAHI GLASS COMPANY, LIMITED
Patent: WO2006/123563 A1, 2006 ;
Location in patent: Page/Page column 9-10 ;
反应条件
potassium hydroxide in water
T=75 - 85°C; P=3000.3 Torr; Inert atmosphereAutoclave;
参考文献
Daikin Industries, Ltd.
Patent: EP2305626 A1, 2011 ;
Location in patent: Page/Page column 14-15 ;
反应条件
chlorine
T=31°C; 7 h; Irradiation;
参考文献
Brace,N.O.
Journal of Organic Chemistry, 1961 , vol. 26, p. 4005 - 4010
反应条件
chlorine
Irradiation.UV-Licht;
参考文献
Du Pont de Nemours and Co.
Patent: US2842601 , 1957 ;
反应条件
chlorine fluorosulfate in dichloro difluoro methane
0.666667 h; Heating;
参考文献
Fokin, A. V; Studnev, Yu. N.; Rapkin, A. I.; Pasevina, K. I.; Potarina, T. M.; Verenikin, O. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1980 , vol. 29, p. 1684 - 1688
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1980 , # 10 p. 2369 - 2374
反应条件
potassium hydroxide in benzene
T=80°C; 1 h;
参考文献
Shilin, S. V.; Florensova, O. N.; Chernov, N. F.; Voronkov, M. G.
J. Gen. Chem. USSR (Engl. Transl.), 1991 , vol. 61, # 8.2 p. 1838 - 1840,1697 - 1699
