2-甲基-2-硝基-1-丙醇合成路线 (共 35 条)
参考文献
Bulletin de l'Academie Polonaise des Sciences, Serie des Sciences Chimiques, , vol. 25, p. 185 - 191
Industrial and Engineering Chemistry, , vol. 32, p. 891
Industrial and Engineering Chemistry, , vol. 32, p. 35
反应条件
5 palladium on charcoal; hydrogen in methanol T=100°C; P=3102.97 Torr; 10 h; Reagent/catalystTemperature;
参考文献
WO2013/133925 A1, ;
Paragraph 0019; 0021; 0022; 0023; 0024 ;
反应条件
5 palladium on charcoal; hydrogen in methanol T=80°C; P=3102.97 Torr; 10 h; SolventTime;
参考文献
WO2013/133925 A1, ;
Paragraph 0020; 0021; 0025 ;
反应条件
5 palladium on charcoal; hydrogen; DTPA-41 in water T=50 - 100°C; P=26618.1 Torr; 3.41667 h; Autoclave;
参考文献
ANGUS CHEMICAL COMPANY; MOORE, David, W.; GREEN, George, D.
Patent: WO2013/133925 A1, 2013 ;
Location in patent: Paragraph 0026 ;
反应条件
triethylamine T=60 - 85°C; 5 h;
参考文献
WO2012/44508 A1, ;
Page/Page column 11-12 ;
反应条件
1: 2-Bromo-2-nitropropane With indium in tetrahydrofuran 0.333333 h; Sonication; 2: formaldehyd in tetrahydrofuran 4 h; Sonication;
参考文献
Soengas, Raquel G.; Estevez, Amalia M.
Synlett, 2010 , # 17 p. 2625 - 2627
参考文献
Journal of the Chemical Society, , p. 1767
参考文献
Journal of the American Chemical Society, , vol. 72, p. 2069
反应条件
T=260.4°C; P=49.5 Torr; Kinetics; Further Variations:PressuresTemperaturesalso in the presence of free radical inhibitors;
参考文献
Dominguez, Rosa Maria; Herize, Armando; Rotinov, Alexandra; Alvarez-Aular, Alvaro; Visbal, Gonzalo; Chuchani, Gabriel
Journal of Physical Organic Chemistry, 2004 , vol. 17, # 5 p. 399 - 408
反应条件
toluene-4-sulfonic acid; xylene unter Entfernen des entstehenden Methanols;
参考文献
Marans; Zelinski
Journal of the American Chemical Society, 1950 , vol. 72, p. 2125