反应条件
1: 1.) pyridine / 1.) a) 0 deg C, overnight, b) 70 deg C, 3 h, 2.) a) 0 deg C, 1 h, b) RT, overnight 2: 95 percent / 1 N NaOH / ethanol / 3 h / 60 °C 3: 30 percent / LiN3 / ethanol / 2 h / Heating 4: 65 percent / DAST / benzene / 2 h / Ambient temperature View Scheme
参考文献
Van Rompaey, Philippe; Nauwelaerts, Koen; Vanheusden, Veerle; Rozenski, Jef; Munier-Lehmann, Helene; Herdewijn, Piet; Van Calenbergh, Serge
European Journal of Organic Chemistry, 2003 , # 15 p. 2911 - 2918
