Reynolds; Evans
Journal of the American Chemical Society, 1938 , vol. 60, p. 2559
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Stacey
Journal of the Chemical Society, 1939 , p. 1529
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Helferich; Moog; Juenger
Chemische Berichte, 1925 , vol. 58, p. 880
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane
0 deg C to room temperature, overnight;
参考文献
Coe, Diane M.; Parry, David M.; Roberts, Stanley M.; Storer, Richard
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 10 p. 2373 - 2378
in n-heptane
byproducts: CO; under Ar or N2, exclusion of light, stirred for 10 min at room temp.; observed by IR, removal of solvent in vac., extn. (toluene), VCl3 sepd. by filtration, soln. evapd. to dryness in vac. at room temp., washed with n-heptane (C2Ph6);
