1: 1-hydroxy-2-(1-methyl)-propylbenzene With iPr2NCHEt2; (-)-Tetramisole in tetrahydrofuran
T=-78°C; 0.5 h; Molecular sieveInert atmosphereResolution of racemate;
2: triphenyl-silyl chloride in tetrahydrofuran
T=-78°C; 48 h; Inert atmosphereResolution of racemate; optical yield given as percent eeenantioselective reaction;
Gilman et al.
Journal of the American Chemical Society, 1950 , vol. 72, p. 1689
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Gmelin Handbook: Si: MVol.C, 26, page 80 - 82
