lithium amide in tetrahydrofuran T=-78 - 20°C; Inert atmosphere;
参考文献
Al-Rafia, S. M. Ibrahim; Lummis, Paul A.; Ferguson, Michael J.; McDonald, Robert; Rivard, Eric
Inorganic Chemistry, 2010 , vol. 49, # 20 p. 9709 - 9717
1: 1-hydroxy-2-(1-methyl)-propylbenzene With iPr2NCHEt2; (-)-Tetramisole in tetrahydrofuran T=-78°C; 0.5 h; Molecular sieveInert atmosphereResolution of racemate; 2: triphenyl-silyl chloride in tetrahydrofuran T=-78°C; 48 h; Inert atmosphereResolution of racemate; optical yield given as percent eeenantioselective reaction;
Higashiya, Seiichiro; Chung, Woo Jin; Lim, Dong Sung; Ngo, Silvana C.; Kelly IV, William H.; Toscano, Paul J.; Welch, John T.
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