Sedel'nikova, V. N.; Lopatin, M. A.; Sennikov, P. G.; Shikova, O. B.; Terman, L. M.
Journal of General Chemistry USSR (English Translation), 1984 , vol. 54, p. 1404 - 1408
Zhurnal Obshchei Khimii, 1984 , vol. 54, p. 1579 - 1583
Reiff et al.
Journal of Organometallic Chemistry, 1968 , vol. 15, p. 247
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Gmelin Handbook: Sn: Org.Verb.1, 1.1.1.16.1.1, page 141 - 147
Lesbre
Bulletin de la Societe Chimique de France, 1935 , vol. <5>2, p. 1195
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Chambers; Scherer
Journal of the American Chemical Society, 1926 , vol. 48, p. 1057
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Krause; Pohland
Chemische Berichte, 1924 , vol. 57, p. 540
in methanol refluxed for 6 h; cooled, filtered, extn. of solid with hot C6H6 (isolation of Ph4Sn fro benzene sol. fraction), filtrate evapd. to dryness, extd. with chloroform, crystd. overnight, filtered and dried in vacuo, recrystd. from C6H6, elem. anal.;
参考文献
Deb, Barun Kanti; Ghosh, Amiya Kanti
Canadian Journal of Chemistry, 1987 , vol. 65, p. 1241 - 1246
Lesbre
Bulletin de la Societe Chimique de France, 1935 , vol. <5>2, p. 1195
Full Text Show Details
Chambers; Scherer
Journal of the American Chemical Society, 1926 , vol. 48, p. 1057
Full Text Show Details
Krause; Pohland
Chemische Berichte, 1924 , vol. 57, p. 540
ammonium chloride; zinc in tetrahydrofuran; water Ph3SnOH is dissolved in THF and added to THF/H2O (NH4Cl saturated) mixt. with excess of zinc powder under stirring, reaction needs 1-1.5 h for completion, THF is removed, residue is treated with chloroform; extn. (chloroform), evapd., crystd. (ethanol);
