1: 2-hydroxy-3-propyl methacrylate With 4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane
T=-25°C; Inert atmosphere;
2: methacrylic acid anhydride T=20°C; 20 h; Inert atmosphere;
参考文献
Blanazs, Adam; Madsen, Jeppe; Battaglia, Giuseppe; Ryan, Anthony J.; Armes, Steven P.
Journal of the American Chemical Society, 2011 , vol. 133, # 41 p. 16581 - 16587