1H-吡唑并[3,4-c]吡啶-3-胺合成路线 （共 7 条）
反应条件
hydrogen; palladium on activated charcoal in ethanol P=1520 Torr;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2398 - 2404
反应条件
hydrazine hydrate in ethanol 4 h; Heating;
参考文献
Organic Preparations and Procedures International, , vol. 29, # 5 p. 577 - 579
反应条件
1: concd. sulfuric acid; nitric acid / 95 °C 2: aq. hydrochloric acid; stannous chloride / Heating View Scheme
参考文献
Heterocycles, , vol. 51, # 7 p. 1661 - 1667
反应条件
1: 80 percent / NaN3 / dimethylformamide / 6.5 h / 90 - 100 °C 2: 87 percent / N2H4*H2O / ethanol / 4 h / Heating View Scheme
参考文献
Organic Preparations and Procedures International, , vol. 29, # 5 p. 577 - 579
反应条件
1: Et3N / tetrahydrofuran / 1 h / 0 °C 2: NH3 / tetrahydrofuran / 1.5 h / 0 °C 3: 96 percent / POCl3 / 2.5 h / Heating 4: 80 percent / NaN3 / dimethylformamide / 6.5 h / 90 - 100 °C 5: 87 percent / N2H4*H2O / ethanol / 4 h / Heating View Scheme
参考文献
Organic Preparations and Procedures International, , vol. 29, # 5 p. 577 - 579
反应条件
1: 96 percent / POCl3 / 2.5 h / Heating 2: 80 percent / NaN3 / dimethylformamide / 6.5 h / 90 - 100 °C 3: 87 percent / N2H4*H2O / ethanol / 4 h / Heating View Scheme
参考文献
Organic Preparations and Procedures International, , vol. 29, # 5 p. 577 - 579
反应条件
1: 97 percent / sodium nitrite, aq. sulphuric acid / 0.5 h 2: 94 percent / 60percent hydrobromic acid / 0.33 h / Heating View Scheme
参考文献
Chapman, David; Hurst, Jim
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2398 - 2404
