2-（3溴苯基）-1-苯基-1H-苯并咪唑合成路线 （共 8 条）
反应条件
triethylamine; trichlorophosphate in 1,4-dioxane; dichloromethane; water
参考文献
NITTO DENKO CORPORATION
Patent: US2011/62386 A1, 2011 ;
反应条件
triethylamine; trichlorophosphate in 1,4-dioxane; dichloromethane; water
参考文献
Nitto Denko Corporation
Patent: US2012/16449 A1, 2012 ;
反应条件
1: With trichlorophosphate in 1,4-dioxane T=115°C; 2 h; 2: With sodium hydrogencarbonate in 1,4-dioxane; dichloromethane; water T=20°C;
参考文献
WO2011/34967 A1, ;
Page/Page column 27-28 ;
反应条件
Na2S2O5 in N,N-dimethyl-formamide T=100°C; 0.1 h; Microwave irradiation;
参考文献
Secci, Daniela; Bolasco, Adriana; D'Ascenzio, Melissa; Della Sala, Flavio; Yanez, Matilde; Carradori, Simone
Journal of Heterocyclic Chemistry, 2012 , vol. 49, # 5 p. 1187 - 1195
反应条件
1.1: triethylamine / dichloromethane / 19 h / 20 °C 2.1: trichlorophosphate / 1,4-dioxane / 2 h / 115 °C 2.2: 20 °C View Scheme
反应条件
1.1: triethylamine / dichloromethane / 19 h / 20 °C 2.1: trichlorophosphate / 1,4-dioxane / 2 h / 115 °C 2.2: 20 °C View Scheme
反应条件
potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane
T=80°C; 17 h; Inert atmosphere;
参考文献
NITTO DENKO CORPORATION; ZHENG, Shijun; SISK, David, T.; HARDING, Brett, T.; CAYAS, Jensen; LI, Sheng; MOCHIZUKI, Amane; CHAE, Hyun, Sik; KHAN, Sazzadur, Rahman; MA, Liping; BOTTGER, Rebecca
Patent: WO2011/34967 A1, 2011 ;
Location in patent: Page/Page column 27-28 ;
反应条件
potassium acetate in dichloromethane
参考文献
NITTO DENKO CORPORATION
Patent: US2011/62386 A1, 2011 ;
Title/Abstract Full Text Show Details
Nitto Denko Corporation
Patent: US2012/16449 A1, 2012 ;
