2-[(苯基硫醇)甲基]-2-环戊烯-1-酮合成路线 （共 6 条）
反应条件
triethylamine in ethanol 110 h; Heating;
参考文献
Cohen, Theodore; Kosarych, Zenyk; Suzuki, Kunio; Yu, Lin-Chen
Journal of Organic Chemistry, 1985 , vol. 50, # 16 p. 2965 - 2968
反应条件
in N,N-dimethyl-formamide T=25°C; 0.5 h;
参考文献
Tamura, Rui; Katayama, Hitoshi; Watabe, Ken-Ichiro; Suzuki, Hitomi
Tetrahedron, 1990 , vol. 46, # 21 p. 7557 - 7568
反应条件
1: 76 percent / 1.) aq. NaOH, 2.) Adogen 464 / benzene; toluene / 0.5 h / 0 °C 2: 1.) Co2(CO)8, 2.) trimethylamine N-oxide dihydrate / 1.) petroleum ether, RT, 4 h, 2.) benzene, MeOH, 35 atm, 40 deg C, 24 h View Scheme
参考文献
Tetrahedron, , vol. 52, # 21 p. 7391 - 7420
反应条件
in N,N-dimethyl-formamide 0.5 h; Ambient temperature;
参考文献
Tamura, Rui; Katayama, Hitoshi; Watabe, Ken-Ichiro; Suzuki, Hitomi
Tetrahedron, 1990 , vol. 46, # 21 p. 7557 - 7568
反应条件
dicobalt octacarbonyl; trimethylamine-N-oxide 1.) petroleum ether, RT, 4 h, 2.) benzene, MeOH, 35 atm, 40 deg C, 24 h; Yield given. Multistep reaction;
参考文献
Tetrahedron, , vol. 52, # 21 p. 7391 - 7420
反应条件
benzaldehyde; cesium fluoride
1.) CH3CN, RT, 2 h, 2.) CH3CN, 1 h; Yield given. Multistep reaction;
参考文献
Cohen, Theodore; Kosarych, Zenyk; Suzuki, Kunio; Yu, Lin-Chen
Journal of Organic Chemistry, 1985 , vol. 50, # 16 p. 2965 - 2968
