反应条件
1: 36 percent / 4-(dimethylamino)pyridine, pyridine / CH2Cl2 / 24 h / Ambient temperature
2: 45 percent / sodium azide / dimethylformamide / 30 h / 80 - 90 °C
3: 0.7 g / H2 / Raney Ni / ethanol / 1 h / 258.6 Torr
View Scheme
参考文献
Trybulski, E.J.; Benjamin, L.; Vitone, S.; Walser, A.; Fryer, R. Ian
Journal of Medicinal Chemistry, 1983 , vol. 26, # 3 p. 367 - 372
