1: ethyl phenylsulphonylacetate With sodium hydride in tetrahydrofuran T=20°C; 0.166667 h; 2: o-(trimethylsilyl)phenyl triflate; acrylic acid methyl ester With potassium fluoride; 18-crown-6 ether in tetrahydrofuran T=65°C; Further stages. Title compound not separated from byproducts.;
参考文献
Huang, Xian; Xue, Jian
Journal of Organic Chemistry, 2007 , vol. 72, # 10 p. 3965 - 3968
1: ethyl phenylsulphonylacetate With sodium hydride in tetrahydrofuran T=20°C; 0.166667 h; 2: o-(trimethylsilyl)phenyl triflate; acrylic acid methyl ester With potassium fluoride; 18-crown-6 ether in tetrahydrofuran T=65°C; Further stages. Title compound not separated from byproducts.;
参考文献
Huang, Xian; Xue, Jian
Journal of Organic Chemistry, 2007 , vol. 72, # 10 p. 3965 - 3968
