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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
76056-08-1
合成路线
(共 3 条)
76056-08-1
→
反应条件
70957-04-9
+
76056-13-8
+
76056-12-7
反应条件
in neat (no solvent) T=250°C; 0.166667 h; In the presence of Ag(1+) lower temperature;
参考文献
Ikeda, Masazumi; Ohno, Kazunori; Takahashi, Masami; Uno, Toshiko; Tamura, Yasumitsu; Kido, Masaru
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 741 - 748
74422-05-2
→
反应条件
76056-08-1
反应条件
<b>Multi-step reaction with 3 steps<br /> </b>1: 88 percent / aq. sodium hydroxide / ethanol / 1 h / 50 °C<br />2: 26 percent / pyridine, copper(II) acetate, lead tetra-acetate / benzene / 1 h / Heating<br />3: 1.) lithium aluminium hydride; 2.) pyridine / 1.) ether, room temperature, 15 min; 2.) room temperature<br /> <br />
参考文献
Ikeda, Masazumi; Ohno, Kazunori; Takahashi, Masami; Uno, Toshiko; Tamura, Yasumitsu; Kido, Masaru Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 741 - 748
74422-11-0
→
反应条件
76056-08-1
反应条件
<b>Multi-step reaction with 2 steps<br /> </b>1: 26 percent / pyridine, copper(II) acetate, lead tetra-acetate / benzene / 1 h / Heating<br />2: 1.) lithium aluminium hydride; 2.) pyridine / 1.) ether, room temperature, 15 min; 2.) room temperature<br /> <br />
参考文献
Ikeda, Masazumi; Ohno, Kazunori; Takahashi, Masami; Uno, Toshiko; Tamura, Yasumitsu; Kido, Masaru Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 741 - 748