2’,4’,5-三羟基-7-甲氧基-6-(3-甲基-1-丁烯基)-3-(3-甲基-2-丁烯基)黄酮合成路线 （共 13 条）
反应条件
1.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 °C
1.2: 2 h / 0 - 20 °C
2.1: ethanethiol; n-butyllithium / N,N,N',N',N'',N''-hexamethylphosphoric triamide / 2 h / 0 - 70 °C / |Inert atmosphere
3.1: ethanethiol; tin(ll) chloride / acetonitrile / 20 °C
View Scheme
参考文献
Zhang, Wen-Jing; Wu, Jing-Fang; Zhou, Peng-Fei; Wang, Yang; Hou, Ai-Jun
Tetrahedron, 2013 , vol. 69, # 29 p. 5850 - 5858
反应条件
1.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 °C
1.2: 2 h / 0 - 20 °C
2.1: ethanethiol; n-butyllithium / N,N,N',N',N'',N''-hexamethylphosphoric triamide / 2 h / 0 - 70 °C / |Inert atmosphere
View Scheme
参考文献
Zhang, Wen-Jing; Wu, Jing-Fang; Zhou, Peng-Fei; Wang, Yang; Hou, Ai-Jun
Tetrahedron, 2013 , vol. 69, # 29 p. 5850 - 5858
反应条件
1: ethanethiol; n-butyllithium / N,N,N',N',N'',N''-hexamethylphosphoric triamide / 2 h / 0 - 70 °C / |Inert atmosphere
2: ethanethiol; tin(ll) chloride / acetonitrile / 20 °C
View Scheme
参考文献
Zhang, Wen-Jing; Wu, Jing-Fang; Zhou, Peng-Fei; Wang, Yang; Hou, Ai-Jun
Tetrahedron, 2013 , vol. 69, # 29 p. 5850 - 5858
