potassium hydroxide in ethylene glycol dimethyl ether Heating;
参考文献
Artamkina, O. B.; Kramarova, E. P.; Shipov, A. G.; Baukov, Yu. I.; Macharashvili, A. A.; et al.
Russian Journal of General Chemistry, 1993 , vol. 63, # 10.2 p. 1590 - 1597
Zhurnal Obshchei Khimii, 1993 , vol. 63, # 10 p. 2289 - 2301
Baukov, Yu. I.; Kramarova, E. P.; Shipov, A. G.; Oleneva, G. I.; Artamkina, O. B.; et al.
J. Gen. Chem. USSR (Engl. Transl.), 1989 , vol. 59, # 1.2 p. 127 - 145,110 - 125
1: CH2Cl2 / -80 °C
2: CH2Cl2 / -80 deg C -> 20 deg C -> -80 deg C
View Scheme
参考文献
Albanov, A. I.; Baukov, Yu. I.; Voronkov, M. G.; Kramarova, E. P.; Larin, M. F.; Pestunovich, V. A.
J. Gen. Chem. USSR (Engl. Transl.), 1983 , vol. 53, # 1 p. 246 - 248,216 - 217
1730 in dichloromethane
-80 deg C -> 20 deg C -> -80 deg C; Title compound not separated from byproducts;
参考文献
Albanov, A. I.; Baukov, Yu. I.; Voronkov, M. G.; Kramarova, E. P.; Larin, M. F.; Pestunovich, V. A.
J. Gen. Chem. USSR (Engl. Transl.), 1983 , vol. 53, # 1 p. 246 - 248,216 - 217
in dichloromethane
-80 deg C -> 20 deg C -> -80 deg C; Title compound not separated from byproducts;
参考文献
Albanov, A. I.; Baukov, Yu. I.; Voronkov, M. G.; Kramarova, E. P.; Larin, M. F.; Pestunovich, V. A.
J. Gen. Chem. USSR (Engl. Transl.), 1983 , vol. 53, # 1 p. 246 - 248,216 - 217
