反应条件
1.1: KO-t-Bu / tetrahydrofuran / 0.25 h / 0 °C
1.2: 92 percent / tetrahydrofuran / 6 h / 0 °C
2.1: 99 percent / aq. HCl / methanol; CH2Cl2 / 12 h / 25 °C
3.1: 90 percent / K2CO3 / acetone / 3 h / Heating
4.1: 73 percent / meta-chloroperoxybenzoic acid; NaHCO3 / CH2Cl2 / 6 h / 25 °C
5.1: 52 percent / KO-t-Bu / dimethylformamide / -57 °C
View Scheme
参考文献
Nicolaou; Snyder, Scott A.; Huang, Xianhai; Simonsen, Klaus B.; Koumbis, Alexandros E.; Bigot, Antony
Journal of the American Chemical Society, 2004 , vol. 126, # 32 p. 10162 - 10173
