反应条件
1: 79 percent / 80percent m-chloroperoxybenzoic acid / CH2Cl2 / 12 h / Ambient temperature
2: 84 percent / various solvent(s) / 50-60 degC, 20 min, rt. 20 h
3: cc. HCl, hydrogen / 10percent palladium on carbon / methanol / 3 h / 760 Torr
4: α,α-dichloromethyl methyl ether / 0.17 h / 50 °C
View Scheme
参考文献
Kubo, Akinori; Nakahara, Shinsuke; Iwata, Ryoichi; Takahashi, Katsuhiro; Arai, Tadashi
Tetrahedron Letters, 1980 , vol. 21, p. 3207 - 3208
