in various solvent(s) 50-60 degC, 20 min, rt. 20 h;

暂无反应条件数据

1: 89 percent / zinc / 0.5 h / Ambient temperature 2: 79 percent / 80percent m-chloroperoxybenzoic acid / CH2Cl2 / 12 h / Ambient temperature 3: 84 percent / various solvent(s) / 50-60 degC, 20 min, rt. 20 h View Scheme

1: cc. HCl, hydrogen / 10percent palladium on carbon / methanol / 3 h / 760 Torr 2: α,α-dichloromethyl methyl ether / 0.17 h / 50 °C View Scheme