1: 72 percent / Ph3PCl2 / acetonitrile / 2.5 h / Ambient temperature 2: 79 percent / LiAlH4 / diethyl ether / 17.5 h / Heating 3: 69 percent / Na 4: 50 percent / AlCl3 / CH2Cl2 / 6.25 h / 0 °C 5: H2 / 5percent Pd-C / ethanol View Scheme
参考文献
Fleming, Ian; Pearce, Andrew
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2485 - 2489
1: 72 percent / Ph3PCl2 / acetonitrile / 2.5 h / Ambient temperature
2: 79 percent / LiAlH4 / diethyl ether / 17.5 h / Heating
3: 69 percent / Na
4: 10 percent / AlCl3 / CH2Cl2 / 6.25 h / 0 °C
View Scheme
参考文献
Fleming, Ian; Pearce, Andrew
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2485 - 2489
