(S)-4-异丙基噻唑烷-2-硫合成路线 （共 12 条）
反应条件
potassium hydroxide 40 h; Reflux;
参考文献
Morales, Edwuin Hander Rios; Roman, Cristina Arbelo; Thomann, Jens Oliver; Meier, Chris
European Journal of Organic Chemistry, 2011 , # 23 p. 4397 - 4408
反应条件
carbon disulfide; potassium hydroxide in water T=100°C; 16 h;
参考文献
Delaunay, Dominique; Toupet, Loic; Corre, Maurice Le
Journal of Organic Chemistry, 1995 , vol. 60, # 20 p. 6604 - 6607
反应条件
in tetrahydrofuran T=80°C; 0.333333 h;
参考文献
Chen, Ning; Jia, Weiyi; Xu, Jiaxi
European Journal of Organic Chemistry, 2009 , # 33 p. 5841 - 5846
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane T=20°C; 15 h; Inert atmosphere;
参考文献
Organic Syntheses, , vol. 86, p. 81 - 91
反应条件
1H-imidazole in dichloromethane 18 h;
参考文献
Tetrahedron, , vol. 58, # 32 p. 6561 - 6576
反应条件
potassium hydroxide in ethanol; water T=70°C; 6 h; Yield given. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 50, # 24 p. 7283 - 7292
反应条件
1: 62 percent / 1 N Na2CO3 / H2O / 0.25 h / 100 °C 2: 80 percent / CS2, 1N KOH / H2O / 16 h / 100 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 60, # 20 p. 6604 - 6607
反应条件
1.1: Sn(OTf)2; N-ethylpiperidine / CH2Cl2 / 4 h / -50 °C 1.2: CH2Cl2 / 14 h / -78 - -50 °C 2.1: 91 percent / imidazole / CH2Cl2 / 18 h View Scheme
参考文献
Tetrahedron, , vol. 58, # 32 p. 6561 - 6576
反应条件
1.1: titanium tetrachloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 2.58 h / -83 - -50 °C / Inert atmosphere 1.2: 2.08 h / -78 °C / Inert atmosphere 2.1: 4-(N,N-dimethlyamino)pyridine; triethylamine / dichloromethane / 15 h / 20 °C / Inert atmosphere View Scheme
参考文献
Organic Syntheses, , vol. 86, p. 81 - 91
反应条件
pyridine in dichloromethane T=20°C; 2 h; Inert atmosphere;
参考文献
Yang, Zhen; Zhang, Bingbin; Zhao, Gaoyuan; Yang, Juan; Xie, Xingang; She, Xuegong
Organic Letters, 2011 , vol. 13, # 21 p. 5916 - 5919
