反应条件
1: 76 percent / Ti(OiPr)4 / 16 h / 120 - 130 °C
2: 96 percent / MnO2 / CH2Cl2 / 0.17 h / Ambient temperature
3: 86 percent / ethyl acetate / 6 h / Ambient temperature
5: 1.) hydrogen, 2.) MnO2 / 1.) Pd(OH)2 on carbon / 1.) ethyl acetate, 15 h, 50 psi, 2.) CH2Cl2, 30 min
6: 95 percent / aq. NaOH / 0.5 h / Ambient temperature
7: 87 percent / 2.) Et3N / CH2Cl2 / 1.) 30 min, 2.) 30 min
8: 53 percent / aq. NaOH / Ra-Ni / 0.17 h / Heating
View Scheme
参考文献
McKenzie, Thomas C.; Choi, Woo-Baeg
Synthetic Communications, 1989 , vol. 19, # 9-10 p. 1523 - 1532
