反应条件
1: hydrogen / 10percent Pd(C) / aq. ethanol
2: 63 percent / DIBAL-H / 1.) -40 deg C, 1.0 h, 2.) 0 deg C, 0.5 h
3: 71 percent / Et3N, 4-N,N-dimethylaminopyridine
View Scheme
参考文献
Caine, Drury; Smith, Troy L. Jr.
Journal of the American Chemical Society, 1980 , vol. 102, # 25 p. 7568 - 7570
