4,4-二甲基-1-戊烯合成路线 （共 69 条）
参考文献
Edmundson, R. S.; Forth, C. I.
Phosphorus and Sulfur and the Related Elements, 1980 , vol. 8, p. 315 - 320
反应条件
OH radical; oxygen; nitrogen(II) oxide T=22.84°C; P=735 Torr; Kinetics;
参考文献
Journal of Physical Chemistry A, , vol. 114, # 18 p. 5810 - 5816
参考文献
Whitmore; Homeyer
Journal of the American Chemical Society, 1933 , vol. 55, p. 4558
反应条件
OH radical; oxygen; nitrogen(II) oxide T=22.84°C; P=735 Torr; Kinetics;
参考文献
Journal of Physical Chemistry A, , vol. 114, # 18 p. 5810 - 5816
反应条件
1: Ozonolyse
View Scheme
参考文献
Whitmore; Homeyer
Journal of the American Chemical Society, 1933 , vol. 55, p. 4558
反应条件
Ascaridole; hydrogen bromide
参考文献
Whitmore; Homeyer
Journal of the American Chemical Society, 1933 , vol. 55, p. 4558
Full Text Show Details
Mallinckrodt Chem.Works
Patent: US2151252 , 1935 ;
参考文献
Whitmore; Homeyer
Journal of the American Chemical Society, 1933 , vol. 55, p. 4558
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Kharasch; Hannum; Gladstone
Journal of the American Chemical Society, 1934 , vol. 56, p. 244
反应条件
1: 65 percent / formic acid, hydrogen peroxide
2: 70 percent / periodic acid / H2O; methanol
3: 23 percent / calcium oxide / H2O / 1.) 3 h, room temperature, 2.) 35 h, 70-80 deg C
4: 79 percent / triethylphosphite, triethylamine / ethanol / Heating
5: 86 percent / sulphuryl chloride / CHCl3 / 2 h
View Scheme
参考文献
Edmundson, R. S.; Forth, C. I.
Phosphorus and Sulfur and the Related Elements, 1980 , vol. 8, p. 315 - 320
反应条件
diethyl ether; bromine
T=-5°C;
参考文献
Whitmore; Homeyer
Journal of the American Chemical Society, 1933 , vol. 55, p. 4558
Full Text Show Details
Mallinckrodt Chem.Works
Patent: US2135064 , 1935 ;
Full Text Show Details
Mallinckrodt Chem.Works
Patent: US2151252 , 1936 ;
