in methanol-d4 T=30°C; 192 h; various solvents; Product distribution;
参考文献
Cokley, Teresa M.; Harvey, Peta J.; Marshall, Raymond L.; McCluskey, Adam; Young, David J.
Journal of Organic Chemistry, 1997 , vol. 62, # 7 p. 1961 - 1964
in acetonitrile dissolved acylquinone and allylstannane stood for 10 min under Ar; concentrated; column chromy. (silica gel); eluted (hexane/ether); NMR; IR; mass spectra; elem. anal.;
参考文献
Maruyama; Matano
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 12 p. 3877 - 3885
in chloroform-d1; dichloromethane-d2 CDCl3/CD2Cl2 = 1:1 at 0.5 M at -80°C; signals ((13)C-NMR) for (CH3)4Sn were visible at -20°C, upon recooling to -80°C redistribution of the allyl groups; (13)C-NMR, the identical spectrum could be obtained by reaction of Me4Sn and (allyl)4Sn with BF3*OEt2 (-80/+20/-80°C);
参考文献
Denmark,S.E.; Wilson,T.; Willson,T.M.
Journal of the American Chemical Society, 1988 , vol. 110, p. 984
dibenzoyl peroxide in hexane Irradiation (UV/VIS); mixt. of stannane, dithiol and benzoyl peroxide in hexane irradiated with UV light for 50 h at -50 to -70°C under stirring; solvent removed under reduced pressure at room temp.; residue passed through silica column with C6H6 as eluent;
参考文献
Shcherbakov; Grigor'eva; Kurskii
Russian Journal of General Chemistry, 2000 , vol. 70, # 6 p. 902 - 906
