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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
76202-52-3
合成路线
（共 9 条）
882503-47-1
→
反应条件
76202-52-3
反应条件
methoxybenzene; trifluoroacetic acid 24 h; Heating;
参考文献
Lamblin, Marc; Couture, Axel; Deniau, Eric; Grandclaudon, Pierre
Tetrahedron, 2006 , vol. 62, # 12 p. 2917 - 2921
882503-45-9
→
反应条件
76202-52-3
反应条件
1.1: n-BuLi / tetrahydrofuran; hexane / 0.25 h / -78 °C 1.2: 70 percent / hexane; tetrahydrofuran / 2 h / -78 - 20 °C 2.1: 91 percent / anisole; trifluoroacetic acid / 24 h / Heating View Scheme
参考文献
Lamblin, Marc; Couture, Axel; Deniau, Eric; Grandclaudon, Pierre
Tetrahedron, 2006 , vol. 62, # 12 p. 2917 - 2921
882503-48-2
→
反应条件
76202-52-3
反应条件
1: 92 percent / sodium borohydride / methanol / 0.5 h / 20 °C 2: 73 percent / NaOH / diethyl ether; H2O / 0.5 h / 0 °C 3: 63 percent / n-BuLi / hexane; tetrahydrofuran / 0.83 h / -90 - -40 °C 4: 91 percent / anisole; trifluoroacetic acid / 24 h / Heating View Scheme
参考文献
Lamblin, Marc; Couture, Axel; Deniau, Eric; Grandclaudon, Pierre
Tetrahedron, 2006 , vol. 62, # 12 p. 2917 - 2921
882503-46-0
→
反应条件
76202-52-3
反应条件
1: 73 percent / NaOH / diethyl ether; H2O / 0.5 h / 0 °C 2: 63 percent / n-BuLi / hexane; tetrahydrofuran / 0.83 h / -90 - -40 °C 3: 91 percent / anisole; trifluoroacetic acid / 24 h / Heating View Scheme
参考文献
Lamblin, Marc; Couture, Axel; Deniau, Eric; Grandclaudon, Pierre
Tetrahedron, 2006 , vol. 62, # 12 p. 2917 - 2921
882503-44-8
→
反应条件
76202-52-3
反应条件
1: 63 percent / n-BuLi / hexane; tetrahydrofuran / 0.83 h / -90 - -40 °C 2: 91 percent / anisole; trifluoroacetic acid / 24 h / Heating View Scheme
参考文献
Lamblin, Marc; Couture, Axel; Deniau, Eric; Grandclaudon, Pierre
Tetrahedron, 2006 , vol. 62, # 12 p. 2917 - 2921
3490-05-9
→
反应条件
76202-52-3
反应条件
1.1: 82 percent / bromine; potassium acetate / 16 h / 20 °C 2.1: n-BuLi / tetrahydrofuran; hexane / 0.25 h / -78 °C 2.2: 70 percent / hexane; tetrahydrofuran / 2 h / -78 - 20 °C 3.1: 91 percent / anisole; trifluoroacetic acid / 24 h / Heating View Scheme
参考文献
Lamblin, Marc; Couture, Axel; Deniau, Eric; Grandclaudon, Pierre
Tetrahedron, 2006 , vol. 62, # 12 p. 2917 - 2921
56008-63-0
→
反应条件
76202-52-3
反应条件
1: toluene / 3 h / Heating 2: 92 percent / sodium borohydride / methanol / 0.5 h / 20 °C 3: 73 percent / NaOH / diethyl ether; H2O / 0.5 h / 0 °C 4: 63 percent / n-BuLi / hexane; tetrahydrofuran / 0.83 h / -90 - -40 °C 5: 91 percent / anisole; trifluoroacetic acid / 24 h / Heating View Scheme
参考文献
Lamblin, Marc; Couture, Axel; Deniau, Eric; Grandclaudon, Pierre
Tetrahedron, 2006 , vol. 62, # 12 p. 2917 - 2921
882503-43-7
→
反应条件
76202-52-3
反应条件
1: 91 percent / anisole; trifluoroacetic acid / 24 h / Heating View Scheme
参考文献
Lamblin, Marc; Couture, Axel; Deniau, Eric; Grandclaudon, Pierre
Tetrahedron, 2006 , vol. 62, # 12 p. 2917 - 2921
78388-10-0
→
反应条件
76202-52-3
反应条件
1: 91 percent / anisole; trifluoroacetic acid / 24 h / Heating View Scheme
参考文献
Lamblin, Marc; Couture, Axel; Deniau, Eric; Grandclaudon, Pierre
Tetrahedron, 2006 , vol. 62, # 12 p. 2917 - 2921
