1: 73 percent / (CF3CO)2O, H2O2, Mo(CO)6 / trifluoroacetic acid; CH2Cl2 / 0 deg C -> room temperature 2: Al-Hg, H2O / tetrahydrofuran 3: tetrahydrofuran; methanol / 0.13 h / 0 °C View Scheme

1: Al-Hg, H2O / tetrahydrofuran 2: tetrahydrofuran; methanol / 0.13 h / 0 °C View Scheme

in tetrahydrofuran; methanol T=0°C; 0.133333 h;