反应条件
1: 1.) n-BuLi / 1.) THF, -78 degC, 3 h; 2.) THF, -78 degC, 0.5 h, allowed to warm to room temp. for 15 h
2: 57 percent / Raney-Ni / ethanol / 6 h / Heating
3: 97 percent / LiAlH4 / tetrahydrofuran / 1 h / Ambient temperature
View Scheme
参考文献
Tomioka, Kiyoshi; Ishiguro, Tsuneo; Iitaka, Yoichi; Koga, Kenji
Tetrahedron, 1984 , vol. 40, # 8 p. 1303 - 1312
