三甲基-(4-三甲基锡烷基萘-1-基)锡烷合成路线 (共 2 条)
反应条件
magnesium; 1,4-dihalogenonaphthalene in tetrahydrofuran
the aromatic halogeno-compd. was added to the soln. of Mg and trimethylchloro-compd., refluxed for several d; hydrolysed with dild. HCl, extd. with ether, dried over Na2SO4, the solvent evapd., the product recrystd. from methanol; elem. anal.;
参考文献
Kaim, Wolfgang; Tesmann, Holger; Bock, Hans
Chemische Berichte, 1980 , vol. 113, # 10 p. 3221 - 3234
反应条件
in tetrahydrofuran
chromy., distn., elem. anal.;
参考文献
Kitching, William; Olszowy, Henry A.; Schott, Inge; Adcock, William; Cox, D. P.
Journal of Organometallic Chemistry, 1986 , vol. 310, p. 269 - 284