3,7-二甲基-4H-苯并[1,4]噻嗪-2-羧酸乙酯合成路线 （共 7 条）
反应条件
0.05 h; microwave irradiation;
参考文献
Khairnar, Bhikan J; Salunke, Rahul S; Patil, Premchand B; Patil, Sanjay A; Kapade, Rajeshwar J; Girase, Pravin S; Chaudhari, Bhata R
E-Journal of Chemistry, 2012 , vol. 9, # 1 p. 318 - 322
反应条件
aluminum oxide in chloroform
0.1 h; microwave irradiation;
参考文献
Paul; Gupta; Loupy; Rani; Dandia
Synthetic Communications, 2001 , vol. 31, # 5 p. 711 - 717
反应条件
piperidine in tetrahydrofuran
2 h; Reflux;
参考文献
Khairnar, Bhikan J.; Girase, Pravin S.; Chaudhari
Oriental Journal of Chemistry, 2013 , vol. 29, # 1 p. 285 - 289
反应条件
1: NaOH / H2O / Heating
2: 50 percent / dimethylsulfoxide / 1 h / Heating
View Scheme
参考文献
Gupta, R. R.; Ojha, K. G.; Kalwania, G. S.; Kumar, M.
Heterocycles, 1980 , vol. 14, # 8 p. 1145 - 1149
反应条件
T=30°C; 0.05 h; Neat (no solvent)Microwave irradiation;
参考文献
Kalwania; Chomal; Choudhary, Savita
Asian Journal of Chemistry, 2011 , vol. 23, # 11 p. 5133 - 5136
反应条件
1.1: bromine; acetic acid / 2.5 h / 5 °C
1.2: Heating
2.1: sodium hydroxide / water
3.1: hydrazine hydrate; N,N-dimethyl-formamide / 0.01 h / Neat (no solvent); Microwave irradiation
4.1: 0.05 h / 30 °C / Neat (no solvent); Microwave irradiation
View Scheme
参考文献
Kalwania; Chomal; Choudhary, Savita
Asian Journal of Chemistry, 2011 , vol. 23, # 11 p. 5133 - 5136
反应条件
1: hydrazine hydrate; N,N-dimethyl-formamide / 0.01 h / Neat (no solvent); Microwave irradiation
2: 0.05 h / 30 °C / Neat (no solvent); Microwave irradiation
View Scheme
参考文献
Kalwania; Chomal; Choudhary, Savita
Asian Journal of Chemistry, 2011 , vol. 23, # 11 p. 5133 - 5136
