(S)-O-甲基-A-苯乙胺合成路线 （共 13 条）
反应条件
5 Pd(II)/C(eggshell); hydrogen in methanol T=60°C; P=11251.1 Torr; 24 h; optical yield given as percent ee;
参考文献
Nugent, Thomas C.; Negru, Daniela E.; El-Shazly, Mohamed; Hu, Dan; Sadiq, Abdul; Bibi, Ahtaram; Umar, M. Naveed
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 2085 - 2092
反应条件
hydrogen; ammonium formate; palladium on activated charcoal in methanol Heating;
参考文献
Bringmann, Gerhard; Geisler, Joerg-Peter; Geuder, Torsten; Kuenkel, Georg; Kinzinger Lioba
Liebigs Annalen der Chemie, 1990 , # 8 p. 795 - 805
反应条件
1: 1) p-TsOH, 2) H2, Raney nickel / 1) toluene, reflux, 2) EtOH, 5 bar, RT, 24h 2: 93 percent / H2, ammonium formate / 10percent Pd-C / methanol / Heating View Scheme
参考文献
Liebigs Annalen der Chemie, , # 8 p. 795 - 805
反应条件
1: With N-(1-(R)-phenylethyl)-oxalamic acid in acetone Heating; 2: With hydrogenchloride
参考文献
Balint, Jozsef; Schindler, Jozsef; Egri, Gabriella; Hanusz, Miklos; Marthi, Katalin; Juvancz, Zoltan; Fogassy, Elemer
Tetrahedron Asymmetry, 2004 , vol. 15, # 21 p. 3401 - 3405
反应条件
hydrogen; ammonium formate; palladium on activated charcoal in methanol Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Liebigs Annalen der Chemie, , # 8 p. 795 - 805
反应条件
palladium hydroxide on carbon; hydrogen T=55°C; P=15001.5 Torr; 48 h;
参考文献
Synthesis (Germany), , vol. 45, # 2 art. no. SS-2012-Z0768-FA, p. 153 - 166
参考文献
Tetrahedron Asymmetry, , vol. 7, # 6 p. 1539 - 1542
反应条件
1: titanium(IV) isopropylate / isopropanol acetate / 0.5 h / Inert atmosphere 2: Pd/Al2O3; hydrogen / isopropanol acetate / 36 h / 35 °C / 15001.5 Torr 3: hydrogen; palladium(II) oxide hydrate / methanol / 48 h / 55 °C / 15001.5 Torr View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 353, # 11-12 p. 2085 - 2092
反应条件
1: sodium hydroxide / water; ethyl acetate 2: 5 Pd(II)/C(eggshell); hydrogen / methanol / 24 h / 60 °C / 11251.1 Torr View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 353, # 11-12 p. 2085 - 2092
反应条件
sodium hydroxide in dichloromethane; water
参考文献
Advanced Synthesis and Catalysis, , vol. 353, # 11-12 p. 2085 - 2092
