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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
76290-79-4
合成路线
（共 8 条）
126920-24-9
→
反应条件
76290-79-4
反应条件
ammonium formate; palladium on activated charcoal in methanol 15 h; Heating;
参考文献
Kiguchi, Toshiko; Kuninobu, Naoko; Takahashi, Yoshiko; Yoshida, Yukiyo; Naito, Takeaki; Ninomiya, Ichiya
Synthesis, 1989 , # 10 p. 778 - 781
66-83-1
5-甲氧基色胺盐酸盐
+
98-88-4
苯甲酰氯
→
反应条件
76290-79-4
反应条件
potassium carbonate in dichloromethane; water T=20°C; 2 h;
参考文献
Cheve, Gwenael; Duriez, Patrick; Fruchart, Jean-Charles; Teissier, Elisabeth; Poupaert, Jacques; Lesieur, Daniel
Medicinal Chemistry Research, 2002 , vol. 11, # 7 p. 361 - 379
126920-23-8
→
反应条件
76290-79-4
反应条件
1: 76 percent / Br2 / acetic acid / 0.5 h / Ambient temperature 2: 79 percent / CuI, Na / dimethylformamide / 2 h / Heating 3: 90 percent / HCOONH4*5H2O / 10percent Pd-C / methanol / 15 h / Heating View Scheme
参考文献
Kiguchi, Toshiko; Kuninobu, Naoko; Takahashi, Yoshiko; Yoshida, Yukiyo; Naito, Takeaki; Ninomiya, Ichiya
Synthesis, 1989 , # 10 p. 778 - 781
126920-26-1
→
反应条件
76290-79-4
反应条件
1: 79 percent / CuI, Na / dimethylformamide / 2 h / Heating 2: 90 percent / HCOONH4*5H2O / 10percent Pd-C / methanol / 15 h / Heating View Scheme
参考文献
Kiguchi, Toshiko; Kuninobu, Naoko; Takahashi, Yoshiko; Yoshida, Yukiyo; Naito, Takeaki; Ninomiya, Ichiya
Synthesis, 1989 , # 10 p. 778 - 781
69001-12-3
+
19501-58-7
4-甲氧基苯肼盐酸盐
→
反应条件
76290-79-4
反应条件
in ethanol; water; acetic acid Heating;
参考文献
Shono, Tatsuya; Matsumura, Yoshihiro; Kanazawa, Takenobu
Tetrahedron Letters, 1983 , vol. 24, # 12 p. 1259 - 1262
19501-58-7
4-甲氧基苯肼盐酸盐
+
68471-55-6
→
反应条件
76290-79-4
反应条件
in ethanol; water; acetic acid Cyclization; Fischer synthesis; 0.333333 h; Heating;
参考文献
Marais, Wilhelmina; Holzapfel, Cedric W.
Synthetic Communications, 1998 , vol. 28, # 19 p. 3681 - 3691
98-88-4
苯甲酰氯
→
反应条件
76290-79-4
反应条件
1: 67 percent / N-ethyldiisopropylamine / benzene / 0.33 h / Heating 2: 85 percent / acetic acid; ethanol; H2O / 0.33 h / Heating View Scheme
参考文献
Marais, Wilhelmina; Holzapfel, Cedric W.
Synthetic Communications, 1998 , vol. 28, # 19 p. 3681 - 3691
3389-54-6
苯基(1-吡咯烷基)甲酮
→
反应条件
76290-79-4
反应条件
1: 80 percent / methoxylation by anodic oxidation (C rods, (C2H5)4NOTs) 2: 87 percent / acetic acid; ethanol; H2O / Heating View Scheme
参考文献
Shono, Tatsuya; Matsumura, Yoshihiro; Kanazawa, Takenobu
Tetrahedron Letters, 1983 , vol. 24, # 12 p. 1259 - 1262
