17-(对甲苯磺酰基氧基)十七烷酸合成路线 （共 6 条）
反应条件
1: NaOEt / ethanol; diethyl ether / 48 h / Ambient temperature
2: 48percent HBr / H2O / 4 h / 120 - 150 °C
3: 54 percent / LiNH2, Fe(NO3)3 / tetrahydrofuran; NH3 / 20 h
4: H2 / PtO2 / diethyl ether
5: pyridine / 0 °C
View Scheme
参考文献
Riche, Francoise; Mathieu, Jean-Paul; Vincens, Maurice; Bardy, Andre; Comet, Michel; Vidal, Michel
Bulletin de la Societe Chimique de France, 1984 , vol. 2, # 1-2 p. 49 - 55
反应条件
1: 54 percent / LiNH2, Fe(NO3)3 / tetrahydrofuran; NH3 / 20 h
2: H2 / PtO2 / diethyl ether
3: pyridine / 0 °C
View Scheme
参考文献
Riche, Francoise; Mathieu, Jean-Paul; Vincens, Maurice; Bardy, Andre; Comet, Michel; Vidal, Michel
Bulletin de la Societe Chimique de France, 1984 , vol. 2, # 1-2 p. 49 - 55
反应条件
1: 48percent HBr / H2O / 4 h / 120 - 150 °C
2: 54 percent / LiNH2, Fe(NO3)3 / tetrahydrofuran; NH3 / 20 h
3: H2 / PtO2 / diethyl ether
4: pyridine / 0 °C
View Scheme
参考文献
Riche, Francoise; Mathieu, Jean-Paul; Vincens, Maurice; Bardy, Andre; Comet, Michel; Vidal, Michel
Bulletin de la Societe Chimique de France, 1984 , vol. 2, # 1-2 p. 49 - 55
反应条件
1: H2 / PtO2 / diethyl ether
2: pyridine / 0 °C
View Scheme
参考文献
Riche, Francoise; Mathieu, Jean-Paul; Vincens, Maurice; Bardy, Andre; Comet, Michel; Vidal, Michel
Bulletin de la Societe Chimique de France, 1984 , vol. 2, # 1-2 p. 49 - 55
反应条件
in pyridine
T=0°C; Yield given;
参考文献
Riche, Francoise; Mathieu, Jean-Paul; Vincens, Maurice; Bardy, Andre; Comet, Michel; Vidal, Michel
Bulletin de la Societe Chimique de France, 1984 , vol. 2, # 1-2 p. 49 - 55
反应条件
sodium iodide in acetone
2 h; Heating; Yield given;
参考文献
Riche, Francoise; Mathieu, Jean-Paul; Vincens, Maurice; Bardy, Andre; Comet, Michel; Vidal, Michel
Bulletin de la Societe Chimique de France, 1984 , vol. 2, # 1-2 p. 49 - 55
